HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-ethyl-1H-1,2,4-triazole-5-acetate → HCID 66828604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-ethyl-1H-1,2,4-triazole-5-acetate | HCID 16463050 | — |
| Reactant | HCID 58188985 | HCID 58188985 | — |
| Product | HCID 66828604 | HCID 66828604 | 19% |
Reaction Steps
Prepared using the same procedure described in Example 275 from (S)-3-benzyl-1-(3-cyclobutyloxy-4-methoxy-phenyl)-piperazine and (5-ethyl-2H-[1,2,4]triazol-3-yl)-acetic acid ethyl ester with heating for 15 days to afford the title compound as tan solid (60 mg, 19%). LC/MS (Method B) 3.22 min, [M+1]+ 490.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927546B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-5da0c26bab5642fe88c223d36f14f4a3 |
| Source note | uspto-grants-2015_01 |