HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-bromo-3-nitro- → 3-Nitrophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-bromo-3-nitro- | HCID 11457 | — |
| Reactant | Cesium hydroxide | HCID 62750 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | 3-Nitrophenol | HCID 11137 | 78% |
Reaction Steps
Following general mode A, 1-bromo-3-nitrobenzene (202 mg, 1.0 mmol) was reacted with cesium hydroxide to give the expected product in the form of a red solid with a yield of 78% (eluent: ethyl acetate/heptane 20:80).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927779B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-5316ac43e426400d8c2e63fab4b49074 |
| Source note | uspto-grants-2015_01 |