HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 67548928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | Ethyl 5-methyl-1H-imidazole-2-carboxylate | HCID 24974466 | — |
| Product | HCID 67548928 | HCID 67548928 | 82.1% |
Reaction Steps
The same operation as in Example (1c) was performed using ethyl 5-methyl-1H-imidazole-2-carboxylate obtained in Example (5a) (0.50 g, 3.23 mmol) and NCS (0.44 g, 3.25 mmol), to obtain 0.50 g of the title compound as a white solid (82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927588B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-ba1da1aa692f45ee90161a371a08174b |
| Source note | uspto-grants-2015_01 |