HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Iodosuccinimide → ethyl 5-ethyl-4-iodo-1H-imidazole-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | Ethyl 5-ethyl-1H-imidazole-2-carboxylate | HCID 14990237 | — |
| Product | ethyl 5-ethyl-4-iodo-1H-imidazole-2-carboxylate | HCID 68405791 | 100% |
Reaction Steps
The same operation as in Example (1c) was performed using ethyl 5-ethyl-1H-imidazole-2-carboxylate obtained by the method described in Example (1b) (0.20 g, 1.19 mmol) and NIS (0.29 g, 1.31 mmol), to obtain 0.35 g of the title compound as a pale yellow solid (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927588B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-2901921a7aad49369cc805db6bdba32f |
| Source note | uspto-grants-2015_01 |