HuagongsheHuagongshe Chemistry Print Report · For research reference only
cis(+/-)-3-(tert-Butoxycarbonyl)amino-1-(diphenylmethyl)-2-ethylazetidine → cis(+/-)-3-(tert-Butoxycarbonyl)amino-2-ethylazetidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | cis(+/-)-3-(tert-Butoxycarbonyl)amino-1-(diphenylmethyl)-2-ethylazetidine | HCID 86648819 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | cis(+/-)-3-(tert-Butoxycarbonyl)amino-2-ethylazetidine | HCID 86648820 | 79% |
Reaction Steps
The same operation as in Example (234e) was performed using cis(±)-3-(tert-butoxycarbonyl)amino-1-(diphenylmethyl)-2-ethylazetidine obtained in Example (235e) (154 mg, 0.42 mmol) and 10% Pd/C (30 mg), to obtain 66 mg of the title compound as a white solid (79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927588B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-177e7e3a0665403b873de4cd572fc87b |
| Source note | uspto-grants-2015_01 |