Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1425449Generated: November 1, 2026

HCID 86648860, compound → Ammonium formate

https://huagongshe.com/reaction/1425449

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86648860HCID 86648860—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductAmmonium formateHCID 27239232,033.3%
ProductHCID 86648859HCID 86648859—

Reaction Steps

The same operation as in Example (90d) was performed using methyl cis(±)-3-(4-{benzyl[(benzyloxy)carbonyl]amino}-3-methoxypiperidin-1-yl)-2-fluorobenzoate obtained in Example (263a) (31 mg, 0.06 mmol), a 10% palladium-carbon catalyst (20 mg), ammonium formate (39 mg, 0.61 mmol) and methanol (4 mL), to obtain the title compound. The resulting compound was used for the next reaction without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08927588B2
Source datasetuspto-grants-2015_01
ORD IDord-1efc17b348ee48b9876dc57fc65e2977
Source noteuspto-grants-2015_01