Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1425560Generated: November 1, 2026

Terephthaloyl chloride → HCID 131731243, compound

https://huagongshe.com/reaction/1425560

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTerephthaloyl chlorideHCID 7488—
ReactantP-PhenylenediamineHCID 7814—
ReactantHCID 20556968HCID 20556968—
ProductHCID 131731243HCID 131731243—

Reaction Steps

The present invention is related to a process which performs the polymerization of 5(6)-amino-2-(p-aminophenyl)benzimidazole, para-phenylenediamine and terephthaloyl dichloride at high solids (7 weight percent or greater) in NMP/CaCl2 or DMAC/CaCl2, isolates the copolymer crumb, dissolves the isolated copolymer crumb in concentrated sulfuric acid to form a liquid crystalline solution, and spins the solution into fibers. By “solids” it is meant the ratio of the mass of copolymer to the total mass of the solution, that is, the mass of the copolymer plus solvent.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08932501B2
Source datasetuspto-grants-2015_01
ORD IDord-e173d4eed78c486fbafe9ee1ec3db16c
Source noteuspto-grants-2015_01