HuagongsheHuagongshe Chemistry Print Report · For research reference only
Terephthaloyl chloride → HCID 131731243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Terephthaloyl chloride | HCID 7488 | — |
| Reactant | P-Phenylenediamine | HCID 7814 | — |
| Reactant | HCID 20556968 | HCID 20556968 | — |
| Product | HCID 131731243 | HCID 131731243 | — |
Reaction Steps
The present invention is related to a process which performs the polymerization of 5(6)-amino-2-(p-aminophenyl)benzimidazole, para-phenylenediamine and terephthaloyl dichloride at high solids (7 weight percent or greater) in NMP/CaCl2 or DMAC/CaCl2, isolates the copolymer crumb, dissolves the isolated copolymer crumb in concentrated sulfuric acid to form a liquid crystalline solution, and spins the solution into fibers. By “solids” it is meant the ratio of the mass of copolymer to the total mass of the solution, that is, the mass of the copolymer plus solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08932501B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-e173d4eed78c486fbafe9ee1ec3db16c |
| Source note | uspto-grants-2015_01 |