Carbazole → HCID 71059533, compound

Participants

Reaction Steps

General experimental procedure for carbazole formation was followed. Reaction was performed on a 8.9 mg scale of 2-(4-(3-fluoropropyl)phenyl)-5-methyl-3-nitropyridine. Isolated 3.6 mg (45%) of T793 as a white solid. 1H NMR (CD3OD): δ 8.48 (1H, d, J=1.6 Hz), 8.39 (1H, d, J=1.6 Hz), 8.21 (1H, d, J=8.4 Hz), 7.55 (1H, d, J=1.6 Hz), 7.34 (1H, d, J=8.4, 1.6 Hz), 4.52 (1H, t, J=6.0 Hz), 4.40 (1H, t, J=6.0 Hz), 2.97 (2H, t, J=7.6 Hz), 2.68 (3H, s), 2.03-2.15 (2H, m); MS: 243 (M+H+).

Provenance & Evidence