HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic anhydride → HCID 57874358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic anhydride | HCID 7922 | — |
| Reactant | tert-Butyl {3-[4-(3-aminopropoxy)butoxy]propyl}carbamate | HCID 14373549 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57874358 | HCID 57874358 | — |
Reaction Steps
1-(tert-Butoxycarbonylamino)-4,9-dioxa-12-dodecanamine (5.0 g, 16.45 mmol) was dissolved in THF (30 mL), succinic anhydride (1.81 g, 18.1 mmol) in acetonitrile (10 mL) was added and the mixture was heated to 60 C for 4 h, and subsequently stirred at RT overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933021B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-0bc284705f594c6c8b3d96257ae23d54 |
| Source note | uspto-grants-2015_01 |