HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → HCID 67997599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | HCID 67997695 | HCID 67997695 | — |
| Product | HCID 67997599 | HCID 67997599 | 19% |
Reaction Steps
The title compound was prepared from 5-bromo-2-methanesulfonylmethyl-pyridine and 1,2-dibromoethane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 19% of theory; LC (method 3): tR=2.52 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933072B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-6a7f82e1c86949b8bce6047e77f3fff5 |
| Source note | uspto-grants-2015_01 |