HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → HCID 86696142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | Pyridine, 2-bromo-6-[(methylsulfonyl)methyl]- | HCID 59526086 | — |
| Product | HCID 86696142 | HCID 86696142 | 53% |
Reaction Steps
The title compound was prepared from 2-bromo-6-methanesulfonylmethyl-pyridine and 1,2-dibromoethane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 53% of theory; LC (method 3): tR=2.56 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933072B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-6103a4b32fdd4ac1b561931e582e43e0 |
| Source note | uspto-grants-2015_01 |