1,4-Dibromobutane → HCID 67997461, compound

HRID 1425988Notes

Reaction equation

HRID 1425988 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][C:9]#[N:10])=[N:6][CH:7]=1.Br[CH2:12][CH2:13][CH2:14][CH2:15]Br>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2([C:9]#[N:10])[CH2:15][CH2:14][CH2:13][CH2:12]2)=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 80561,4-DibromobutaneHCID 29927881(5-Bromopyridin-2-yl)acetonitrile

Product 1

HCID 67997461HCID 67997461, compoundYield 78%

Procedure

The title compound was prepared from (5-bromo-pyridin-2-yl)-acetonitrile and 1,4-dibromobutane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 78% of theory; Mass spectrum (ESI+): m/z=251/253 (Br) [M+H]+.

Sources & evidence

ORD record
ord-7bd7b318d5d44db7b6f9652682dbdc8c
Source dataset
uspto-grants-2015_01
Patent number
US08933072B2

Reaction notes

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