Phenylacetylene → HCID 50913149, compound

HRID 1426221Notes

Reaction equation

HRID 1426221 reaction equation
Br[C:2]1[CH:3]=[N:4][C:5]2[N:6]([N:8]=[CH:9][N:10]=2)[CH:7]=1.[C:11]1([C:17]#[CH:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([C:17]#[C:18][C:2]2[CH:3]=[N:4][C:5]3[N:6]([N:8]=[CH:9][N:10]=3)[CH:7]=2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 10821PhenylacetyleneHCID 158669806-Bromo[1,2,4]triazolo[1,5-a]pyrimidine

Product 1

HCID 50913149HCID 50913149, compound

Procedure

The title compound, light brown solid, MS: m/e=221.2 (M+H+), can be prepared in accordance with the general method of example 1 from 6-bromo-[1,2,4]triazolo[1,5-a]pyrimidine (example 32, step 1) and phenylacetylene.

Sources & evidence

ORD record
ord-afc99ab448554888ba54c1064a25950e
Source dataset
uspto-grants-2015_01
Patent number
US08933094B2

Reaction notes

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