Phenylacetylene → HCID 53247452, compound
Reaction equation
Br[C:2]1[CH:3]=[CH:4][C:5]2[N:6]([N:8]=[N:9][CH:10]=2)[CH:7]=1.[C:11]1([C:17]#[CH:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([C:17]#[C:18][C:2]2[CH:3]=[CH:4][C:5]3[N:6]([N:8]=[N:9][CH:10]=3)[CH:7]=2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1Participants
3
Procedure
The title compound, light brown solid, MS: m/e=220.3 (M+H+), can be prepared in accordance with the general method of example 1 from 6-bromo-[1,2,3]triazolo[1,5-a]pyridine (example 34, step 1) and phenylacetylene.
Sources & evidence
- ORD record
- ord-ab7fd29005b144c283fc8486b52f6cf1
- Source dataset
- uspto-grants-2015_01
- Patent number
- US08933094B2
Reaction notes
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