Phenylacetylene → HCID 58316717, compound

HRID 1426237Notes

Reaction equation

I[C:2]1[CH:3]=[CH:4][C:5]2[N:6]([N:8]=[C:9]([C:11]([CH3:15])([CH3:14])[CH2:12][OH:13])[N:10]=2)[CH:7]=1.[C:16]1([C:22]#[CH:23])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[CH3:14][C:11]([C:9]1[N:10]=[C:5]2[CH:4]=[CH:3][C:2]([C:23]#[C:22][C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[CH:7][N:6]2[N:8]=1)([CH3:15])[CH2:12][OH:13]

Participants

Reactant 2

HCID 10821Phenylacetylene

HCID 58316701HCID 58316701, compound

Product 1

HCID 58316717HCID 58316717, compound

Procedure

The title compound, a brown solid, MS: m/e=292.0 (M+H+), can be prepared in accordance with the general method of example 1 from 2-(6-iodo-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-2-methyl-propan-1-ol (example 40, step 7) and phenylacetylene.

Sources & evidence

ORD record: ord-ea2f42f7f4a6490ebcf108de8a76ea82
Source dataset: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08933094B2

Reaction notes

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