HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetylene → 2-tert-Butyl-6-phenylethynyl-[1,2,4]triazolo[1,5-a]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetylene | HCID 10821 | — |
| Reactant | 6-Bromo-2-tert-butyl-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 58316704 | — |
| Product | 2-tert-Butyl-6-phenylethynyl-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 53247571 | — |
Reaction Steps
The title compound, a yellow solid, MS: m/e=277.1 (M+H+), can be prepared in accordance with the general method of example 1 from 6-bromo-2-tert-butyl-[1,2,4]triazolo[1,5-a]pyrimidine (example 42, step 1) and phenylacetylene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933094B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-2b110013a9c94895904ea00b41164de3 |
| Source note | uspto-grants-2015_01 |