2-Bromopropanedial → HCID 58316725, compound

HRID 1426253Notes

Reaction equation

HRID 1426253 reaction equation
[N:1]1([C:6]2[NH:10][N:9]=[C:8]([NH2:11])[N:7]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1.[Br:12][CH:13]([CH:16]=O)[CH:14]=O>>[Br:12][C:13]1[CH:14]=[N:11][C:8]2[N:9]([N:10]=[C:6]([N:1]3[CH2:2][CH2:3][CH2:4][CH2:5]3)[N:7]=2)[CH:16]=1

Participants

3

Reactant 2

HCID 749452-BromopropanedialHCID 178509276HCID 178509276, compound

Product 1

HCID 58316725HCID 58316725, compound

Procedure

The title compound, a light red solid, MS: m/e=268.1/270.1 (M+H+), can be prepared in accordance with the general method of example 42, step 1 from 5-pyrrolidin-1-yl-1H-[1,2,4]triazol-3-ylamine (CAS 154956-89-5) and 2-bromomalonaldehyde.

Sources & evidence

ORD record
ord-5aaa31fb9a554a7b9adcf996fed86610
Source dataset
uspto-grants-2015_01
Patent number
US08933094B2

Reaction notes

Loading…