HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzenesulfonyl chloride → HCID 67398941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzenesulfonyl chloride | HCID 9588 | — |
| Reactant | HCID 67396538 | HCID 67396538 | — |
| Product | HCID 67398941 | HCID 67398941 | — |
Reaction Steps
By an operation similar to that in Reference Example 32 and using tert-butyl {[5-(2-fluoropyridin-3-yl)-1H-pyrrol-3-yl]methyl}methylcarbamate (305 mg), and 4-fluorobenzenesulfonyl chloride (292 mg), the title compound was obtained as a colorless oil (yield 436 mg, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933105B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-54ebf262bf4749988016cc36161c098d |
| Source note | uspto-grants-2015_01 |