HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → HCID 69085790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | HCID 20269590 | HCID 20269590 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 69085790 | HCID 69085790 | 87.7% |
Reaction Steps
The 3-(p-tolylthio)benzene-1,2-dicarboxylic acid is slowly added to 18 g of chlorosulfonic acid cooling at 5 and 10° C. with an ice-bath. After 1 hour the mixture is poured in iced water. The precipitate is filtered, washed with water and dried obtaining 1.20 g (87.7%) of 7-methyl-9-oxo-9H-thioxanthene-1-carboxylic acid as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933142B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-9660c8af9b944e27b3a1bcb3cc9acbe9 |
| Source note | uspto-grants-2015_01 |