Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 69085790 | HCID 69085790 | — |
| Catalyst | Toluene | HCID 1140 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86695882 | HCID 86695882 | — |
Reaction Steps
0.21 g (0.78 mmoles) of 7-methyl-9-oxo-9H-thioxanthene-1-carboxylic acid are suspended in 30 ml of toluene containing 2 drops of DMF and 0.35 g of thionyl chloride. After stirring for 1 hour at 80° C. the mass is cooled to room temperature obtaining a yellow solution of 7-methyl-9-oxo-9H-thioxanthene-1-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08933142B2 |
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| Source dataset | uspto-grants-2015_01 |
|---|
| ORD ID | ord-40a5576e99f34f34abadab06044973ba |
|---|
| Source note | uspto-grants-2015_01 |
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