HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 70596896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 86705052 | HCID 86705052 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 70596896 | HCID 70596896 | — |
Reaction Steps
To a solution of the product from step C (20 mg, 0.036 mmol, enantiomer A) in pyridine (5 mL) was added POCl3 (0.05 mL). The mixture was stirred at RT for 2 h. The residue was purified by Combiflash (Mobile phase: MeOH/H2O (0.08% of NH4HCO3) to obtain the title compound. LC/MS m/z=564.0 [M+Na]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933113B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-0a1138ac059044729b679dc31a93c782 |
| Source note | uspto-grants-2015_01 |