HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → Methyl 3-(4-amino-1H-indol-1-yl)-3-(4-chlorophenyl)pentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | tert-Butyl 3-(4-(tert-butoxycarbonylamino)-1H-indol-1-yl)-3-(4-chlorophenyl)pentanoate | HCID 117809455 | — |
| Product | Methyl 3-(4-amino-1H-indol-1-yl)-3-(4-chlorophenyl)pentanoate | HCID 68175795 | — |
Reaction Steps
A mixture of the product of Step F (120 mg, 0.24 mmol) and 4 N HCl/MeOH (2 mL) was stirred at room temperature for 2 h. The volatile was removed in vacuo to give the title compound as colorless oil. LC/MS m/z=357.1[M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933113B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-c65139464ff94b269e12deba4cee1038 |
| Source note | uspto-grants-2015_01 |