Methanol → HCID 86705062, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of the product from Step A (60 mg, 0.140 mmol) in MeOH (3 mL) was added MeONa (15 mg, 0.281 mmol). The mixture was stirred at 120° C. under microwave for 0.5 h. The solution was removed and the residue was purified by PREP-TLC eluting with PE/EA (1/1, v/v) to give the title compound as a colorless amorphous solid. LC/MS m/z=359.1[M+H]+.

Provenance & Evidence