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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1428173Generated: November 1, 2026

Tetrahydrofuran → HCID 82230217, compound

https://huagongshe.com/reaction/1428173

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrahydrofuranHCID 8028—
ReactantHCID 86682822HCID 86682822—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 82230217HCID 82230217102.8%

Reaction Steps

To a mixture of 2-methyl-5-[(E)-2-(4-nitrophenyl)ethenyl]-1,3,4-oxadiazole (2.00 g), tetrahydrofuran (75 mL) and methanol (75 mL) was added palladium-carbon (Pd: 10%, 50% in water, 200 mg), and the mixture was stirred under a hydrogen atmosphere at room temperature for 6 hr. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (1.807 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08937055B2
Source datasetuspto-grants-2015_01
ORD IDord-90f55b3125554750b52c0bc88478e80b
Source noteuspto-grants-2015_01