HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 82230217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 86682822 | HCID 86682822 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 82230217 | HCID 82230217 | 102.8% |
Reaction Steps
To a mixture of 2-methyl-5-[(E)-2-(4-nitrophenyl)ethenyl]-1,3,4-oxadiazole (2.00 g), tetrahydrofuran (75 mL) and methanol (75 mL) was added palladium-carbon (Pd: 10%, 50% in water, 200 mg), and the mixture was stirred under a hydrogen atmosphere at room temperature for 6 hr. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (1.807 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937055B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-90f55b3125554750b52c0bc88478e80b |
| Source note | uspto-grants-2015_01 |