HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethoxy-2-nitroaniline → 4-Ethoxy-1,2-benzenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethoxy-2-nitroaniline | HCID 69229 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Product | 4-Ethoxy-1,2-benzenediamine | HCID 14532 | — |
Reaction Steps
To a mixture of 4-ethoxy-2-nitroaniline (963 mg) and THF/EtOH (1/1, 10 mL) was added 10% Pd/C (281 mg), followed by stirring at room temperature for 3 hours under a hydrogen atmosphere. The reaction mixture was filtered and the filtrate was concentrated under reduced pressure to obtain 4-ethoxybenzene-1,2-diamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937087B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-faef092b683e47b69b1f7daea82df087 |
| Source note | uspto-grants-2015_01 |