1-Bromonaphthalene → HCID 46913279, compound

HRID 1428427Notes

Reaction equation

HRID 1428427 reaction equation
[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1.[C:12](Cl)(=[O:15])[CH:13]=[CH2:14].[Cl-].[Al+3].[Cl-].[Cl-]>>[Br:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([C:12](=[O:15])[CH:13]=[CH2:14])=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 70011-BromonaphthaleneHCID 13140Acryloyl chlorideHCID 6451240Aluminum(III) Chloride

Product 1

HCID 46913279HCID 46913279, compoundYield 4.2%

Procedure

1-bromonaphthalene (0.42 g), acryloyl chloride (0.31 g), and aluminium chloride (0.27 g) were treated in the same manner as described in Example 1 to obtain the title compound (22 mg).

Sources & evidence

ORD record
ord-1a4f92d6157e422595324374d71e2bdc
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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