Benzene → 19847-64-4

HRID 1428443Notes

Reaction equation

HRID 1428443 reaction equation
[CH:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:7](Cl)(=[O:12])/[C:8](=[CH:10]/[CH3:11])/[CH3:9].[Cl-].[Al+3].[Cl-].[Cl-]>ClCCl>[C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)(=[O:12])/[C:8](=[CH:10]/[CH3:11])/[CH3:9]

Participants

5

Reactant 3

HCID 241BenzeneHCID 5325503(2E)-2-Methyl-2-butenoyl chlorideHCID 6451240Aluminum(III) Chloride

Product 1

HCID 599241119847-64-4

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Benzene (1 mL), tigloyl chloride (236 mg), and aluminium chloride (160 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (126 mg).

Workup

  1. additionThe resultant was treated in the same manner

Sources & evidence

ORD record
ord-6b8e1fc032b74c878ed095b493b5e8bc
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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