HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Tert-butyl-m-xylene → 2,6-Dimethyl-4-t-butyl-1-acryloylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Tert-butyl-m-xylene | HCID 7378 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,6-Dimethyl-4-t-butyl-1-acryloylbenzene | HCID 46913482 | — |
Reaction Steps
5-t-butylmetaxylene (0.5 mL), acryloyl chloride (120 mg), and aluminium chloride (150 mg) were reacted in dichloromethane (1.5 mL) at from −40° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (120 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-1f38244b93d54d9a9df49f23e0d57e56 |
| Source note | uspto-grants-2015_01 |