HuagongsheHuagongshe Chemistry Print Report · For research reference only
Veratrole → 2-Propen-1-one, 1-(3,4-dimethoxyphenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Veratrole | HCID 7043 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Propen-1-one, 1-(3,4-dimethoxyphenyl)- | HCID 11171521 | 29.3% |
Reaction Steps
1,2-dimethoxybenzene (135 mg), acryloyl chloride (118 mg), and aluminium chloride (199 mg) were reacted in dichloromethane (1.5 mL) at from −40° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (55 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-d3bd0e0245564a79aeb2cfda9adb82a1 |
| Source note | uspto-grants-2015_01 |