HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Phenylnaphthalene → Acryloyl-1-phenylnaphthalene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Phenylnaphthalene | HCID 11795 | — |
| Edukt | Acryloyl chloride | HCID 13140 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Acryloyl-1-phenylnaphthalene | HCID 86673232 | 125,2% |
Reaktionsschritte
1-phenylnaphthalene (204 mg), acryloyl chloride (200 mg), and aluminium chloride (290 mg) were reacted in dichloromethane (1.5 mL) at from −40° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (323 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08937091B2 |
| Quelldatensatz | uspto-grants-2015_01 |
| ORD ID | ord-d3ef5e2ceed241289f186007c662443e |
| Quellennotiz | uspto-grants-2015_01 |