Formaldehyde → HCID 70926392, compound

HRID 1428468Notes

Reaction equation

HRID 1428468 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=[O:3])[CH3:2].[CH:10]([NH:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)(C)C.[CH2:21]=O.O1[CH2:28][CH2:27]OCC1>>[CH:27]([CH:14]([NH:13][CH2:10][CH2:2][C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=[O:3])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)([CH3:28])[CH3:21]

Participants

5

Reactant 4

HCID 712FormaldehydeHCID 7410AcetophenoneHCID 312751,4-DioxaneHCID 66024Isopropylbenzylamine

Product 1

HCID 70926392HCID 70926392, compound

Procedure

Acetophenone (17 mg), isopropylbenzylamine (149 mg), and paraformaldehyde (39 mg) were reacted in dioxane (0.2 ml) at 150° C. for 2 hours reaction.

Workup

  1. customreaction

Sources & evidence

ORD record
ord-b05f54ce321a4b1e91056e70bbbe893b
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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