HCID 593861, compound → HCID 11030731, compound

HRID 1428471Notes

Reaction equation

HRID 1428471 reaction equation
[CH2:1]([CH:4]([C:6]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[CH:8][CH:7]=1)[OH:5])[CH:2]=[CH2:3].[Cr](Cl)([O-])(=O)=O.[NH+]1C=CC=CC=1>ClCCl>[CH2:1]([C:4]([C:6]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]=[CH:8][CH:7]=1)=[O:5])[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 593861HCID 593861, compoundHCID 178418287HCID 178418287, compound

Product 1

HCID 11030731HCID 11030731, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Allyl-1-naphthylcarbinol (205 mg) and pyridinium chlorochromate (230 mg) were reacted in dichloromethane (2 mL) at room temperature for 4 hours.

Sources & evidence

ORD record
ord-e22c269ac0bf4517a8ed159ebf9908a5
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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