Formaldehyde → HCID 70926749, compound

HRID 1428479Notes

Reaction equation

HRID 1428479 reaction equation
[C:1]([C:4]1[CH:5]=[N:6][CH:7]=[CH:8][CH:9]=1)(=[O:3])[CH3:2].NCC[C:13]1[N:17]=[CH:16][NH:15][CH:14]=1.C=O>O1CCOCC1>[NH:15]1[CH:14]=[CH:13][N:17]=[C:16]1[CH:5]([NH:6][CH2:7][CH2:2][C:1]([C:4]1[CH:5]=[N:6][CH:7]=[CH:8][CH:9]=1)=[O:3])[CH3:4]

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 95893-AcetylpyridineHCID 178419017HCID 178419017, compound

Product 1

HCID 70926749HCID 70926749, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

3-acetylpyridine (6.5 mg), histamine (6 mg), and paraformaldehyde (2 mg) were reacted in dioxane (0.1 ml) at 150° C. for 2 hours.

Sources & evidence

ORD record
ord-c038ed9f6b5742efa7b5d8743c42ba29
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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