Manganese → gamma-Cyclodextrin Manganese

Participants

Reaction Steps

23 g of a manganese-based drier, Manganese CEM-ALL® 12% solution (OM Group, Inc.) was added to the above-noted γ-cylodextrin solution. A brown precipitate formed upon addition of the drier. The mixture was stirred for at least 16 hours. The precipitate was filtered off under reduced pressure. The filtrate was light yellow coloured. The precipitate was dried under reduced pressure (around 19 InHg) at 50-60° C. The FTIR spectrum of the resultant inclusion complex is provided in FIG. 1(d).

Provenance & Evidence