Trifluoroacetic acid → HCID 68590160, compound

Participants

Reaction Steps

Compound 3f was dissolved in DCM (20 ml). Triethyl silane (0.6 ml, 3.75 mmol) and TFA (20 ml) were added. The reaction mixture was stirred at RT for 1.5 h. The solvent was co evaporated with toluene and the crude residue was purified by column chromatography (DCM→DCM/MeOH (90/10)) which gave the title compound, (583 mg, 96%), MS (M+H)+476.

Provenance & Evidence