HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 68589773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 68590234 | HCID 68590234 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 68589773 | HCID 68589773 | 76.7% |
Reaction Steps
A solution of the ethyl ester 17e (0.67 g, 1.1 mmol) in THF/MeOH 1:1 (30 ml) was treated with a 1M solution of LiOH (15 ml) as described in Example 13 step d which gave the title compound, (0.49 g, 76%), (M+H)+581.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937080B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-746d81a4825b4e729534d060bb2a4636 |
| Source note | uspto-grants-2015_01 |