Carbazole → HCID 66883634, compound

HRID 1429307Notes

Reaction equation

[CH:1]1[C:13]2[NH:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][CH:2]=1.F[C:15]1[CH:53]=[CH:52][C:18]([C:19]([C:21]2[CH:22]=[CH:23][C:24]3[N:25]([C:43]4[CH:48]=[CH:47][C:46]([C:49](=[O:51])[CH3:50])=[CH:45][CH:44]=4)[C:26]4[C:31]([C:32]=3[CH:33]=2)=[CH:30][C:29]([C:34](=[O:42])[C:35]2[CH:40]=[CH:39][C:38](F)=[CH:37][CH:36]=2)=[CH:28][CH:27]=4)=[O:20])=[CH:17][CH:16]=1>>[CH:10]1[C:11]2[N:12]([C:15]3[CH:53]=[CH:52][C:18]([C:19]([C:21]4[CH:22]=[CH:23][C:24]5[N:25]([C:43]6[CH:48]=[CH:47][C:46]([C:49](=[O:51])[CH3:50])=[CH:45][CH:44]=6)[C:26]6[C:31]([C:32]=5[CH:33]=4)=[CH:30][C:29]([C:34](=[O:42])[C:35]4[CH:40]=[CH:39][C:38]([N:12]5[C:13]7[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=7[C:6]7[C:11]5=[CH:10][CH:9]=[CH:8][CH:7]=7)=[CH:37][CH:36]=4)=[CH:28][CH:27]=6)=[O:20])=[CH:17][CH:16]=3)[C:13]3[C:5](=[CH:4][CH:3]=[CH:2][CH:1]=3)[C:6]=2[CH:7]=[CH:8][CH:9]=1

Participants

Reactant 2

HCID 6854Carbazole

HCID 66883335HCID 66883335, compound

Product 1

HCID 66883634HCID 66883634, compound

Procedure

1-{4-[3,6-Bis-(4-carbazol-9-yl-benzoyl)-carbazol-9-yl]-phenyl}-ethanone is prepared by the same method as described in example 6.a with an excess amount of carbazole and 1-{4-[3,6-bis-(4-fluoro-benzoyl)-carbazol-9-yl]-phenyl}-ethanone.

Sources & evidence

ORD record: ord-d9e16c3697c74995855653a6786b2632
Source dataset: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08940464B2

Reaction notes

Loading…