HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Allylglycine → Methyl (2R)-2-aminopent-4-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Allylglycine | HCID 6992334 | — |
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Product | Methyl (2R)-2-aminopent-4-enoate | HCID 11446533 | 98% |
Reaction Steps
A solution of (R)-2-aminopent-4-enoic acid (18d) (5 g, 43.5 mmol) in MeOH.HCl (2.4M, 50 mL) was stirred at 70° C. overnight. The mixture was concentrated under reduced pressure to give compound 18e (5.5 g, 98% yield), which was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940722B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-74805e60e5a341f3a98737816ad574a2 |
| Source note | uspto-grants-2015_01 |