Triethylamine → HCID 86677163, compound

Participants

Reaction Steps

To a solution of 30d (2.27 g, 7.62 mmol) and Et3N (2.12 mL, 15.2 mmol), MsCl (1.2 mL, 15.2 mmol) was added dropwise at 0° C. After addition was complete, the reaction was stirred at rt until LC-MS analysis indicated the total consumption of the SM. The solvent was removed and the residue was purified by CC using PE:EA=5:1 as mobile phase to afford the desired product (2.9 g, quant.)

Provenance & Evidence