2-(Tributylstannyl)pyridine → HCID 59631328, compound

Participants

Reaction Steps

Prepared according to Procedure E using 2,4-dichloro-3-methylquinoline (1.038 g, 4.9 mmol), 2-(tributylstannyl)pyridine (2.0 g, 5.4 mmol) and tetrakis(triphenylphosphine)palladium(0) (0.28 g, 0.24 mmol) in toluene (10.00 mL) to afford product as an off-white solid upon purification by precipitation from EtOAc and chromatography on silica gel, eluting with EtOAc gradient in hexane. Mass Spectrum (ESI) m/e=255.1 (M+1).

Provenance & Evidence