HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 59631403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 3-Fluoroaniline | HCID 9742 | — |
| Reactant | Diethyl isopropylmalonate | HCID 12966 | — |
| Product | HCID 59631403 | HCID 59631403 | — |
Reaction Steps
Prepared according to procedure A using 3-fluoroaniline (8.70 mL, 90 mmol), pyridine (10.92 mL, 135 mmol) and diethyl isopropylmalonate (20.02 mL, 99 mmol). The crude was purified by column chromatography (Hexanes:EtOAc, 1:0 to 4:1) to give ethyl 2-(3-fluorophenylcarbamoyl)-3-methylbutanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940724B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-3cc87b49e7b04f938d9320da670e6757 |
| Source note | uspto-grants-2015_01 |