Pyridine → HCID 86611585, compound

Participants

Reaction Conditions

Reaction Steps

An ice cold solution of 0.584 g (6.66 mmol) 4-penten-1-ol and 1.11 ml (14.0 mmol) pyridine in 5 ml DCM is treated with 0.866 ml (6.77 mmol) benzene sulfonyl chloride. After 30 minutes at 0° C. the mixture is stirred overnight at rt. The mixture is diluted with DCM, washed with 5% aqueous citric acid, water and 5% aqueous NaHCO3, dried with sodium sulfate and evaporated, yielding the benzenesulfonic acid pent-4-enyl ester as a colorless oil that is used without further purification.

Provenance & Evidence