HRID1432346

反应详情

EQUATION

反应方程式

HRID 1432346 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 1.5 g of 4-(5,6,7,8-tetrahydroimidazo[1,5-a]pyridin-5-yl)benzoic acid [93178-73-5] in 5 ml of acetic acid is hydrogenated (50 bar) in the presence 0.05 g of Nishimura catalyst at room temperature. The reaction mixture is clarified by filtration, and the filtrate is evaporated. The crude title compound is obtained from the residue.

WORKUP

后处理

  1. customat room temperature
  2. filtrationThe reaction mixture is clarified by filtration
  3. customthe filtrate is evaporated