化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → Methyl 5-bromo-3-methylthiophene-2-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 5-Bromo-3-methylthiophene-2-carboxylic acid | HCID 18176663 | — |
| 生成物 | Methyl 5-bromo-3-methylthiophene-2-carboxylate | HCID 53438912 | — |
反応手順
After thionyl chloride was added to methanol, 5-bromo-3-methylthiophene-2-carboxylic acid was added thereto and the resulting solution was heated and refluxed to obtain methyl 5-bromo-3-methylthiophene-2-carboxylate. EI: 234, 236.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07612108B2 |
| 出典データセット | uspto-grants-2009_11 |
| ORD ID | ord-ee3b2633ffc3488b8fc4da110dcdef8b |
| 出典メモ | uspto-grants-2009_11 |