HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Iodomethyl)cyclopentane → (3S,5S)-3-(Cyclopentylmethyl)-3-methyl-5-phenylmorpholin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Iodomethyl)cyclopentane | HCID 2762531 | — |
| Reactant | (5S)-3-methyl-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one | HCID 57467834 | — |
| Product | (3S,5S)-3-(Cyclopentylmethyl)-3-methyl-5-phenylmorpholin-2-one | HCID 57935240 | — |
Reaction Steps
The compound was prepared according to the procedure outlined in Preparation 1 using (5S)-3-methyl-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one (1 g, 5.28 mmol, see WO-A-02/051983) and (iodomethyl)cyclopentane. The total amount of compound synthesised was 0.426 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07612226B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-558f2c2f0f98440c8da23e4e2696968f |
| Source note | uspto-grants-2009_11 |