HCID 23087108, compound → HCID 57934534, compound

HRID 1433812Notes

Reaction equation

HRID 1433812 reaction equation
NC1(C[O:8]C2C=CC(C#N)=CC=2)CCCC1.[CH3:17][N:18]([CH3:34])[C:19]1([CH2:24][O:25][C:26]2[CH:33]=[CH:32][C:29]([C:30]#N)=[CH:28][CH:27]=2)[CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH3:17][N:18]([CH3:34])[C:19]1([CH2:24][O:25][C:26]2[CH:33]=[CH:32][C:29]([CH:30]=[O:8])=[CH:28][CH:27]=2)[CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

3

Procedure

Synthesized from 4-(1-aminocyclopentylmethoxy)benzonitrile according to an analogous synthetic method to Preparation Example 18, 4-(1-dimethylaminocyclopentylmethoxy)benzonitrile (1.2 g) was used according to an analogous synthetic method to Preparation Example 16 to provide the title compound (1.2 g).

Workup

  1. customwas used according to an analogous synthetic method to Preparation Example 16

Sources & evidence

ORD record
ord-437615b11f6b4e91b6d95fd27088a2ec
Source dataset
uspto-grants-2009_11
Patent number
US07612114B2

Reaction notes

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