HCID 23087111, compound → HCID 57934423, compound

HRID 1433813Notes

Reaction equation

HRID 1433813 reaction equation
NC1(C[O:8]C2C=CC(C#N)=CC=2)CCCC1.[C:17]([C:19]1[CH:39]=[CH:38][C:22]([O:23][CH2:24][C:25]2([NH:30][C:31](=[O:37])[O:32][C:33]([CH3:36])([CH3:35])[CH3:34])[CH2:29][CH2:28][CH2:27][CH2:26]2)=[CH:21][CH:20]=1)#N>>[CH:17]([C:19]1[CH:39]=[CH:38][C:22]([O:23][CH2:24][C:25]2([NH:30][C:31](=[O:37])[O:32][C:33]([CH3:36])([CH3:35])[CH3:34])[CH2:29][CH2:28][CH2:27][CH2:26]2)=[CH:21][CH:20]=1)=[O:8]

Participants

3

Reactant 2

HCID 23087111HCID 23087111, compoundHCID 86605236HCID 86605236, compound

Product 1

HCID 57934423HCID 57934423, compound

Procedure

Synthesized from 4-(1-aminocyclopentylmethoxy)benzonitrile according to an analogous synthetic method to Preparation Example 19, tert-butyl [1-(4-cyanophenoxymethyl)cyclopentyl]carbamate (1.0 g) was used according to an analogous synthetic method to Preparation Example 20 to provide the title compound (688 mg).

Workup

  1. customwas used according to an analogous synthetic method to Preparation Example 20

Sources & evidence

ORD record
ord-9cd22f91e002493abdfec5d36ca2ef5f
Source dataset
uspto-grants-2009_11
Patent number
US07612114B2

Reaction notes

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