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HRID1433862

反应详情

EQUATION

反应方程式

HRID 1433862 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2c(c1)CCC(OS(=O)(=O)C(F)(F)F)=C2
HCID15330256

3,4-Dihydro-6-methoxy-2-naphthalenyl 1,1,1-trifluoromethanesulfonate

C12H11F3O4S

结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1ccc(OC)cc1[N+](=O)[O-]
HCID23087474

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(c1)CCC(c1ccc(OC)cc1[N+](=O)[O-])=C2
HCID23087141

未命名化合物

收率 73.2%

PROCEDURE

实验过程

Synthesized from 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.3 g) and tributyl(4-methoxy-2-nitrophenyl)tin (3.9 g) according to an analogous synthetic method to Preparation Example 77, the title compound (1.7 g) was obtained.

WORKUP

后处理

  1. customaccording to an analogous synthetic method to Preparation Example 77