HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Methoxy-2-tetralone → 6-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Methoxy-2-tetralone | HCID 77785 | — |
| Reactant | 7-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate | HCID 23087446 | — |
| Reactant | Tributyl(4-methoxy-2-nitrophenyl)tin | HCID 23087474 | — |
| Product | 6-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene | HCID 23087535 | — |
Reaction Steps
Synthesized from 7-methoxy-2-tetralone according to an analogous synthetic method to Preparation Example 82 described above, 7-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (3.5 g) and tributyl(4-methoxy-2-nitrophenyl)tin (18 g) were used according to an analogous synthetic method to Preparation Example 77 to provide the title compound (1.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07612114B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-aec3a4cc0fa34e72aa5bd13c7fcc48b3 |
| Source note | uspto-grants-2009_11 |