Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1433936Erstellt: 25. Oktober 2026

6-Methoxy-alpha-tetralone → 7-Methoxy-3-(2-methyl-6-nitrophenyl)-1,2-dihydronaphthalene

https://huagongshe.com/reaction/1433936

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt6-Methoxy-alpha-tetraloneHCID 14112—
Edukt2-Bromo-3-nitrotolueneHCID 231828—
Edukt3-Bromo-7-methoxy-1,2-dihydronaphthaleneHCID 11601147—
Produkt7-Methoxy-3-(2-methyl-6-nitrophenyl)-1,2-dihydronaphthaleneHCID 23087267—

Reaktionsschritte

Synthesized from 6-methoxy-1-tetralone according to an analogous synthetic method to Preparation Example 106, 3-bromo-7-methoxy-1,2-dihydronaphthalene (2.7 g) and 2-bromo-3-nitrotoluene (4.8 g) were used according to an analogous synthetic method to Preparation Example 107 to provide 7-methoxy-3-(2-methyl-6-nitrophenyl)-1,2-dihydronaphthalene (925 mg). This compound (920 mg) was used according to an analogous synthetic method to Example 30 to provide the title compound (740 mg).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07612114B2
Quelldatensatzuspto-grants-2009_11
ORD IDord-55f9d1dee1134589b386cbddb7a92ca3
Quellennotizuspto-grants-2009_11